Physico Mechanical Standards

Physico-Mechanical Standards Division is one of seven R&D Divisions of National Physical Laboratory, India. The division constitutes of mechanical measurement activities involving the parameters of

1. Mass, Volume, Density and Viscosity Standards
2. Length and Dimension Standards
3. Temperature and Humidity Standards
4. Optical Radiation Standard (visible infrared and ultraviolet regions)
5. Force, Torque and Hardness Standards
6. Pressure and Vacuum Standards
7. Acoustic and Ultrasonic Standards
8. Fluid Flow Standards (Water medium only)
9. Shock and Vibration Sensors

The division is responsible to establish, maintain and continually upgrade the National Standards of Measurements related to above said activities and disseminates the standards by providing the apex level calibration services to the industry and institutions of the country and thus ensures the traceability to measurements made by these.

NPL, India is the signatory of the Mutual Recognition Arrangement (MRA) of BIPM and the calibration and measurement capabilities (CMC) of most of the activities are available on BIPM website (www.bipm.org).

The above activities participated in 07 international inter-comparison organized/ coordinated by BIPM and or APMP (Asia Pacific Metrology Program) / RMOs (Regional Metrology Organization of Asian region) regularly.

New measurement facilities were created to disseminate with improved measurement uncertainty to user industries by establishing the following primary/reference standards:

• One kg mass Comparator
• Traceability of the Flick Standard with Laser Interferometer
• Measurement of Type-S & R thermocouples to develop Standards thermocouples in the range
1000-1600 °C
• Variable Temperature blackbody primary standard of spectral radiance
• Vickers Hardness Primary Standard
• Fully automated fluid flow primary standard based on gravimetric method upto 60 K litre/hr.

In order to expedite the process of establishing the network of National Measurement System, the
scientists of this division helped National Accreditation Board for Testing and Calibration Laboratories (NABL)
as the Lead and Technical Assessors in assessing technical capabilities of several laboratories.
In order to maintain the uniformity in measurements capabilities of different industries operating in the
same area, well regulated proficiency testing program was organized in collaboration with NABL.

Length & Dimension Standards Group has developed a new methodology using image processing and wavelet transform is developed to measure the size of the wire sieves and their spacing. Wire sieves are used in pharmaceuticals/chemical industries for filtering the grains of chemical powder.

A new facility for calibration of high temperature noble metal thermocouples has been created in the range from 1000 ºC to 1600 ºC. Now, standard thermocouples of Type-S, R & B could possibly be calibrated in the overall range from 0 to 1600 ºC. The facility was created for the first time in India to provide apex level calibration and traceability to NABL accredited laboratories all over the country.

 

Source based primary standard of spectral radiance in the form of a variable temperature blackbody has been established. This blackbody works in the temperature range of 1800K – 3200K with temperature stability of ± 0.2K. Its emissivity is 0.999, and exhibits radiance uniformity within 0.1%, in the wavelength range 0.2 μm-2.5 μm. The uncertainty in spectral radiance measurement using this blackbody is 0.3-0.5% in the wavelength range 0.2 μm-0.4 μm, and 0.1-0.3% in the wavelength range 0.4 μm-2.5 μm, respectively. The established facility is shown in Fig. 1.3.

The Dead weight force machine in the range 5-50 N developed earlier was extended to a lower range of 1 N using a specially designed hanger made from aluminium alloy. This fully automated machine has been characterised in the range 1 to 20N using 2N, 3N, 5N, 10N and 20N force transducers and typical calibration results are shown in Fig.

 

Vacuum Standards

Characterization of Gas Operated Piston Gauge against UIM, the Nation Primary Standard:

We have evaluated of measurement uncertainty using:

(a) Method of Effective Area Estimation of Piston-Cylinder assembly

Preparation of Uncertainty Budget

Determination of Coverage Factor for the required confidence level

Estimation of expanded uncertainty

Q(0.05 Pa, 0.000828 % of reading) at k=2.

(b) Method of Direct Comparison